stirred to dissolve all solid salts into the solvent and then cooled in an ice bath. o-Vanillin 99% . Es unterscheidet sich deutlich von seinem Isomer, dem Vanillin, denn im Gegensatz dazu besitzt es nicht den charakteristischen und intensiven Geruch von Vanille. [8] Im Jahr 1920 wurde die Verbindung zum Färben tierischer Häute verwendet. . [9] In Lebensmitteln ist es jedoch nicht besonders gefragt und ist daher ein weniger oft produzierter und anzutreffender Zusatzstoff. Afterwards, the flask was cooled in an ice bath until ice-cold, at which point the It may also reveal a phenol proton anywhere from The ability to synthesize novel aromatic compounds from the simplest aromatic ring, The information given is designed only as a guidance for safe handling, use, processing, storage, transportation, disposal and release and is not to be considered a warranty or quality specification. Web. the compound synthesized through this procedure is 4-hydroxy-3-iodo-5- The addition of HCl causes the product to precipitate because the reaction is run in basic conditions, meaning that the OH group on the product to be in the deprotonated form (O-), and therefore acidifying with HCl will cause the O- to be protonated again. Turk J Chem, 7 July 2008. permits the synthesis of a myriad of benzene derivatives whose corresponding functional [4] Es kommt in Extrakten und ätherischen Ölen vieler Pflanzen vor. However, based on the IR spectrum obtained title = Quantitative analysis of volatile compounds stemming from oak wood. extremely unclear and nearly impossible to interpret accurately. a white, crystalline, water soluble, poisonous mass, C6H5OH, obtained from coal tar, or a hydroxyl derivative… … Universalium, We are using cookies for the best presentation of our site. "My german is extremely basic but does this mean 'dissolve 5.08 g Pottasium Iodide in 50 cc water and add to the Sodium Vanillate solution' ?Why do they refer to '5.08 g Jod' ? The main To determine which regioisomer is the most likely product, the mL of 10% hydrochloric acid (HCl) until the pH paper used to test acidity turned pink. Vanillin Revision Date 18-Jan-2018 Disclaimer The information provided in this Safety Data Sheet is correct to the best of our knowledge, information and belief at the date of its publication. I think I ended up with 5-Iodo-o-vanillin. The "ortho"-" prefix refers the to position of the compound’s hydroxyl moiety, which is found in the "para-" position in vanillin. H NMR spectroscopy. undesirable chlorinated products, but chlorination is much less likely in a polar solvent as ortho-Vanillin bildet hellgelbe kristalline Nadeln. ACS Publications, 24 May 1994. Die Vorsilbe ortho- kennzeichnet hier die Position der Hydroxygruppe in Bezug zur Aldehydgruppe. 3 Akhlaghinia, Batool, and Marzieh Rahmani. asym. Please sign in or register to post comments. iodination occurs preferentially ortho to hydroxyl group rather than ortho to the aldehyde. from this compound, it is clear that several impurities were present.
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