Suppliers 8 That should be your O-CH3 peak (very electronegative withdrawing group (oxygen). Press J to jump to the feed. Vanillyl alcohol Biological Activity. M OH 1. I am not an NMR expert, but this has worked for me so far. H H. 3. N Molecular Weight 154.16 . Vanillyl alcohol ≥98%, FG Synonym: 4-Hydroxy-3-methoxybenzyl alcohol, NSC 3993, Vanillyl alcohol CAS Number 498-00-0. H. 8. Vanillyl alcohol is a monomethoxybenzene that is 2-methoxyphenol substituted by a hydroxymethyl group at position 4. When problem solving NMRs, my thought process is this: 1-Identify solvent peak 2-Label all hydrogens groups on my structure. Press question mark to learn the rest of the keyboard shortcuts. Terms & Conditions -, Lead Time: Disclaimer, Copyright © 2013-2020 MOLBASE All Rights Reserved ICP Shanghai 14014220, Lead Time: About Us vanillyl alcohol. Use a NMR spectrum table to identify the locations and assign them accordingly. 2004-09-16. Next peak is the one around 4.6, that one should be the R-CH2-R group near the alcohol. T I was totally lost until you posted this. O. Vanillyl alcohol has been used in trials studying the treatment of Smoking. 6 Please do not post entire problem sets or questions that you haven't attempted to answer yourself. Products : 498-00-0. MDL number MFCD00004659. B 4-Hydroxy-3-methoxybenzyl alcohol. Synonyms: 4-Hydroxy-3-methoxybenzyl alcohol; Benzenemethanol, 4-hydroxy-3-methoxy-; 4-Hydroxy-3-methoxybenzyl Alcohol; 4- … R I am trying to make sense of this NMR spectrum for vanillyl alchohol linked below and I'm completely confused. 690 . Lets start with right-most peak thats around 3.9. It has a role as a plant metabolite. Z Draw Vanillyl Alcohol on your spectrum, and make sure you draw out the hydrogens. 4, NaOH 2. Chemical Encyclopedia Vanillin MW 152.15 C. 8. Business Cooperation Ill PM you if I have any more questions. Partners F C L O Best of luck! X 1 Day, More vanillyl alcohol NMR spectra of reference. CAS No. 9, Home 1 FEMA Number 3737 . 3 Vanillyl alcohol. That should be your O-CH3 peak (very electronegative withdrawing group (oxygen). NaBH. Notice how the three peaks go in a 3:2:1 ratio, characteristic of the number of protons. Draw Vanillyl Alcohol on your spectrum, and make sure you draw out the hydrogens. Next peak is the one around 4.6, that one should be the R-CH2-R group near the alcohol. 2 4 P Chen Z, et al. [1]. Beilstein/REAXYS Number 1910044 . Reduction of Vanillin to Vanillyl Alcohol . 3. U Lets start with right-most peak thats around 3.9. Also please don't use this sub to cheat on your exams!! Contact Us By using our Services or clicking I agree, you agree to our use of cookies. Molecular Formula C 8 H 10 O 3; Average mass 154.163 Da; Monoisotopic mass 154.062988 Da; ChemSpider ID 56139 The last peak, around 7.2, should be the last hydrogen off the ring, on the opposite side of the two i just mentioned. Any tips for how I might go about approaching this problem? Privacy Policy D : A Do you guys have any idea which bands represent which protons? S Q This corresponds to the two adjacent hydrogens off the ring. 7 O + OH OCH. Structure Feel free to PM if you have questions. Vanillyl alcohol View entire compound with free spectra: 4 NMR, 2 FTIR, 2 Raman, and 2 UV-Vis Linear Formula HOC 6 H 3 (OCH 3)CH 2 OH . W 3. Notice the peak is splitting (characteristic of having other protons within three bonds). Names. Additionally, if anyone has any good H NMR proton links I could definitely use the help. It is a member of guaiacols and a member of benzyl alcohols. 5 4- (Hydroxymethyl)-2-methoxyphenol. PubChem Substance ID 24901864. Vanillyl alcohol View entire compound with free spectra: 4 NMR, 2 FTIR, 2 Raman, and 2 UV-Vis Attenuated Total Reflectance Infrared (ATR-IR) Spectrum View the Full Spectrum for FREE! New comments cannot be posted and votes cannot be cast. Here is the link to the spectrum http://imgur.com/N7jWBZZ. Vanillyl alcohol (Vanillic alcohol), derived from vanillin, is a phenolic alcohol and is used as a flavoring agent in foods and beverages [1]. EC Number 207-852-4. Y Thank you so much I really appreciate it. 3. J I 3-Methoxy-4-hydroxybenzyl alcohol. Cookies help us deliver our Services. This is apparently a thing now that people are writing exams from home. K Other names. V Chemical Product Establishing an Artificial Pathway for De Novo Biosynthesis of Vanillyl Alcohol in Escherichia coli. 4-Hydroxy-3-methoxybenzenemethanol. Vanillyl alcohol. The next peak at around 5.6 should be the OH, attached to the CH2 we just discussed. CAS Number Search, Compound Synonyms H O OCH. Council of Europe no. E Preferred IUPAC name. Post your questions about chemistry, whether they're school related or just out of general interest. G The next peak we can look at is the one at 6.8. Vanillic alcohol. 3-Start on one end, and work my way down.
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